Skip to end of metadata
Go to start of metadata

You are viewing an old version of this page. View the current version.

Compare with Current View Page History

« Previous Version 3 Next »

A large number of the probes listed below were purchased separately and re-built for specific projects. Hence, we have a complete electronics/mechanics workshop and related expertise. 


Less-routine spectrometers (all Bruker) 


300 MHz Avance II (3 ch, solid/liquid with 1kW X-amplifier), WB (2006)

Diffusion/microimaging probes, Max temperature 60°C for 10 mm, 80°C for 5mm inserts

Diff25 300MHz WB probe (25G/cm/A).  Z-grad 960 G/cm at Imax=40A, 10 mm and 5 mm rf inserts for 1H and 2H.

Diff60 300MHz WB probe (60 G/cm/A).  Z-grad 3000 G/cm at Imax=50A, 10 mm and 5 mm rf inserts for 1H and 2H.

MIC5 300MHz SB/WB probe (5 G/cm/A). XYZ-grad 300 G/cm at Imax=60A. 1H

MIC2.5 300MHz. Setup includes WB-sized gradient tube with XYZ-gradients, 150 G/cm at Imax=60A (» 2.5 G/cm/A) and SB-sized rf probe head with exchangeable resonators.

Resonators: 2mm 1H (solenoid), 5mm1H (saddle), 10mm 1H  (saddle), 20mm 1H (bird-cage), 30mm1H (bird-cage), 10mm 1H (homebuilt, with extended field of view), 10mm 19F, 10mm 2H.

 

Solution NMR probes

ATM BBF (broad-band and 19F) 5mm SB

Several (>8) different BBI 5mm, BBO 10mm , BBO 5mm probes plus various unconventional/re-built probes from GE, Bradley.


Solid probes

HR-MAS 4mm, max 15 kHz, max 90°C, CP-MAS 4mm, max 15 kHz,  -150°C/+150°C, CP-MAS 7mm, max 7 kHz,  -150°C/+150°C

Static X nuclei, wide range of rf inserts, -150°C/+150°C

 

500 MHz Avance III 3 ch, SB (2007) and 500 MHz Avance HD, SB (2013)

Both spectrometers are solid/liquid, with interchangeable probes (except MAS, on Avance HD)

 

Diffusion/microimaging probes, Max temperature 60°C for 10 mm, 80°C for 5mm inserts if not stated otherwise

DIFF/30 500MHz SB probe (G/cm/A). Z-grad 1800 G/cm at Imax=60A and MIC5 500 SB probe (5 G/cm/A). XYZ 300 G/cm at Imax=60A. 

Both probes have 10mm and 5 mm rf inserts for a wide range of nuclei, also RF inserts also for extended temp range -100°C/+200oC.

 

Solution NMR probes

Several (>10) different BBI 5mm, BBO 10mm , BBO 5mm, TXI (1H/13C/15N) 5mm, TXI (1H/13C/15N) 10mm and a few with unconventional nuclei combinations (such as 19F/1H 5mm).

 

High-temperature probe

High-tem. DUL 1H/13C/2H 5mm, -100°C/+600°C

 

Solid probe

CP-MAS 4mm, max 15kHz, -90°C/+90°C

 

Other less-routine NMR equipment, stand-alone or add-ons

 

NMR Mouse 13 MHz, NMR Mouse 9 kHz, NMR handheld Mouse 13 MHz

Portable console KEA upgraded with 500W amplifier + Potable battery-driven NMR console Magritec

 

Two complete setups (power supply + probes inserts) for electrophoretic NMR

Rapid liquid-liquid and liquid-solid mixing probes inserts

Temperature-jump probe insert

Light-induced kinetics probe (UV/Vis through optical fibre)


1 T horizontal MR system (Aspect Imaging) with a 30 G/cm peak gradient strength. For complex flow studies at the Dept of Mechanics.

 

Spectrometers primarily for high-throughput routine service (all Bruker)

400 MHz Nanobay Avance III HD (2013)

BBO Smart probe 5mm, gradient

BBO 5mm, gradient

1H/13C inverse probe, 5mm, with gradient


400 MHz Nanobay Avance III HD (2013)

BBO Smart probe 5mm, gradient
TXI 1.7 mm H/C/N with gradient

 

500 MHz Avance (2004, partly upgraded since)

BBO 5mm, gradient

BBI 5mm, gradient

 

400 MHz DRX (1999)

5 mm H/BB inverse with Z-grad
5mm H/BB normal without grad
5 mm H/C (dual) normal without grad
5 mm 1H without grad
10 mm H/BB normal without grad
10 mm H/205Tl normal without grad

  • No labels